The role of silver nanoparticles synthesized from Brassica olerace for determination of Aspirin in pharmaceutical samples by standard additions method

Authors

  • Muhammad Ismail College of Energy Dynamics and Mechanical Engineering, North China Electric Power University, Beijing, China Author
  • Wang Xiangke College of Energy Dynamics and Mechanical Engineering, North China Electric Power University, Beijing, China Author
  • Ali H. Reshak Physics Department, College of Science, University of Basrah, Basrah 61004, Iraq Author
  • Dania Ali Charles University Faculty of Medicine, Pilsen 30100, Czech Republic Author
  • Aneeba Amjad Centre of Biotechnology and Microbiology, University of Peshawar, Peshawar 25120, Pakistan Author
  • Qaisar Khan Islamia College Peshawar, Department of Zoology, Peshawar 25120, Khyber Pakhtunkhwa, Pakistan Author
  • Muhammad Ishaq Electrical Engineering Department, COMSATS University Islamabad, Islamabad, 45550, Pakistan Author
  • Abdul Ahad Khan Department of Physics, University of Peshawar, Peshawar 25120, Pakistan Author
  • Zeshan Zada Materials Modeling Lab, Department of Physics, Islamia College University, Peshawar 25120, Pakistan Author

DOI:

https://doi.org/10.56053/7.2.95

Keywords:

Silver nanoparticles, Brassica oleracea, Aspirin

Abstract

In this study, silver nanoparticles (Ag NPs) were prepared from Brassica oleracea (BO) leaflet extract (BO-AgNPs) and applied for to determination of Aspirin in pharmaceutical samples through selective and sensitive spectrophotometric standard additions method. The measurements of UV-Visible, X-ray diffraction (XRD), Fourier transform infrared (FTIR) and scanning electron microscopy (SEM) have been used to confirm the formation of BO-AgNPs, revealing a prominent absorption band at 450 nm, crystallinity, and an agglomerated morphology having an average particle size of 29 nm. Aspirin in Acifein, Aspirin, Acylpyrin and Disprin tablets was determined through the complexation with BO-AgNPs, revealing a linear range of 1-10 mg/10 mL and limit of detection (LOD) as 0.09, 0.46, 0.69 and 0.99 mg/10 mL, respectively. An average percent recovery for four samples were found to be 90, 99, 101 and 99 % and relative standard deviation (RSD) as 1.6, 0.6, 0.3 and 1.4, respectively. The suggested method was successfully used for the quantitative analysis of pharmaceutical tablets, which opens up the possibility that Ag NPs could be used to determine biological molecules when interferences from real samples are present.

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Published

2023-04-15

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How to Cite

The role of silver nanoparticles synthesized from Brassica olerace for determination of Aspirin in pharmaceutical samples by standard additions method. (2023). Experimental and Theoretical NANOTECHNOLOGY, 7(2), 95-110. https://doi.org/10.56053/7.2.95