Nano-ceramics Ti3SiC2 Max phase reinforced single walled carbon nanotubes by spark plasma sintering
DOI:
https://doi.org/10.56053/1.2.49Keywords:
MAX phase, Ti3SiC2, SPSAbstract
Ceramics titanium silicon carbide Ti3SiC2 Max phase was rapidly synthesised and simultaneously consolidated by spark plasma sintering at which the extensive volume expansion occurred as a function of the temperature from ball milled SiC/Ti/C powders with Ti/SiC ratio of 3:1:2. The XRD patterns results were confirmed by FESEM observations and the EDAX analyses. The 3Ti+1.2SiC+0.8C nano-ceramics were processed from 3Ti+1.2SiC+0.8C/SWCNTs powders using spark plasma sintering (SPS) at temperatures of 1100, 1200 and 1300 oC with diting of SWCNTs from 0.0 to 1.0 wt% SWCNTs/Ti3SiC2 nanocomposite. The effects of SWCNTs addition on phases, microstructure and hardness of the nanocomposite were investigated. The best product contained 1.0 wt% CNTs/ Ti3SiC2/TiC which was sintered at 1300 °C, 60 MPa for 10 min The phase composition of the product could be tailored by adjusting the process parameters. The anisotropic hardness was observed in respect to the textured product.
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